반응 #87685

반응 방정식

3-fluoro-4-iodobenzamide

oxalyl chloride

→

desired product

3-fluoro-4-iodobenzoyl isocyanate

용매

EDC

반응 조건

후처리

1. 1
   기타The title compound was prepared

실험 절차

The title compound was prepared according to the procedure described in step-2 of Intermediate-8 by using 3-fluoro-4-iodobenzamide (2.0 g), oxalyl chloride (0.120 mL) and EDC (25 mL) to afford 1.0 g of the desired product.

출처