반응 #87652

ord-20dc6dfe4d63487aa01a19a960959ba1

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The title compound was prepared

실험 절차

The title compound was prepared according to the procedure described in step-1 of Intermediate-61 by using 4-fluoro-3-(trifluoromethyl)aniline (3.0 g, 0.016 mmol), NaNO2 (1.73 g, 0.025 mmol), SnCl2.2H2O (9.39 g, 0.041 mmol) and conc. HCl (100 mL) to afford 2.0 g of the desired product.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US09439890B2uspto-grants-2016_09