반응 #86859

반응 방정식

6,6-dimethyl-5,7-dioxaspiro[2.5]octane-4,8-dione

o-toluidine

→

2-oxo-1-o-tolylpyrrolidine-3-carboxylic acid

수율 91.0%

용매

ethanol

반응 조건

후처리

1. 1
   기타This compound was prepared

실험 절차

This compound was prepared according to general method 1 starting from 6,6-dimethyl-5,7-dioxaspiro[2.5]octane-4,8-dione (0.250 g, 1.47 mmol) and o-toluidine (0.470 mL; 4.41 mmol) in ethanol (3 mL). 2-oxo-1-o-tolylpyrrolidine-3-carboxylic acid 0.292 g (91%) was obtained as a white film.

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