반응 #86648

반응 방정식

Methyl ester

(R)-3-Allylsulfanyl-2-tert-butoxycarbonylamino-propionic acid methyl ester

hydrogen chloride

→

(R)-3-Allylsulfanyl-2-amino-propionic acid methyl ester hydrochloride

용매

1,4-dioxane

반응 조건

후처리

1. 1
   농축before being concentrated in vacuo
2. 2
   기타to yield a white solid, 2.46 g, 100%

실험 절차

Methyl ester 29 (3.20 g, 11.6 mmol) was dissolved in 4M hydrogen chloride in 1,4-dioxane (40 mL). The resultant solution was stirred at rt for 18 h before being concentrated in vacuo to yield a white solid, 2.46 g, 100%.

출처