반응 #8661

ord-bfaaa2dc17da42f6b989cc71db7aee74

반응 방정식

C=CC(=C)C
isoprene
C=CC=C
1,3-butadiene
C=CC(=C)C.C=CC=C
isoprene butadiene

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    workup.ADDITIONcontaining
  2. 2
    기타were consumed after 9 minutes

실험 절차

In this experiment, a 30/70 isoprene-butadiene rubber (IBR) was prepared using a preformed catalyst described in Example 2. The procedure described in Example 3 was utilized in this examples except that a premix containing a 30:70 mixture of isoprene and 1,3-butadiene was used as the monomers. GC analysis of the residual monomer indicated that 90 percent of monomers were consumed after 9 minutes. The polymerization was continued for an additional 21 minutes.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07091150B2uspto-grants-2006_08