반응 #85193

반응 방정식

4-[5-chloro-2-(difluoromethoxy)phenyl]-5-methoxypyridin-2(1H)-one

tert-butyl bromoacetate

potassium carbonate

→

tert-Butyl {4-[5-chloro-2-(difluoromethoxy)phenyl]-5-methoxy-2-oxopyridin-1(2H)-yl}acetate

반응 조건

후처리

1. 1
   기타according to General Method 4B at 100° C

실험 절차

5.43 g (purity 80%, 14.4 mmol) of 4-[5-chloro-2-(difluoromethoxy)phenyl]-5-methoxypyridin-2(1H)-one and 1.2 eq. of tert-butyl bromoacetate in the presence of 1.5 eq. of potassium carbonate were reacted according to General Method 4B at 100° C. Yield: 3.64 g (61% of theory)

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