반응 #85188

ord-e904aa120be84616a2892da6d75764e1

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

139 mg (purity 85%, 0.27 mmol) of tert-butyl 2-[5-chloro-4-(5-chloro-2-cyanophenyl)-2-oxopyridin-1(2H)-yl]-4-methylpentanoate (racemate) were hydrolysed with TFA according to General Method 6A. Yield: 87 mg (84% of theory)

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US09434690B2uspto-grants-2016_09