반응 #84877

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2-(4-chloro-3,5-dimethoxyphenyl)furan

2-ethoxy-N-methoxy-N-methyl-2-(4-morpholinophenyl)acetamide

→

1-(5-(4-Chloro-3,5-dimethoxyphenyl)furan-2-yl)-2-ethoxy-2-(4-morpholinophenyl)ethanone

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후처리

1. 1
   기타Purification by chromatography (60% EtOAc-hexanes)

실험 절차

1-(5-(4-Chloro-3,5-dimethoxyphenyl)furan-2-yl)-2-ethoxy-2-(4-morpholinophenyl)ethanone was prepared from 2-(4-chloro-3,5-dimethoxyphenyl)furan and 2-ethoxy-N-methoxy-N-methyl-2-(4-morpholinophenyl)acetamide according to the procedure used in Example 30. Purification by chromatography (60% EtOAc-hexanes) gave the product as a pale yellow solid (0.127 g, 26% yield). MS: m/z 486.5 [M+H]+.

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