반응 #848

반응 방정식

p-hydroxybenzoic acid

decanoic acid chloride

pyridine

→

p-decanoyloxybenzoic acid

용매

water

반응 조건

후처리

1. 1
   추출an organic layer was extracted with dichloromethane
2. 2
   세척The organic layer was washed with 1N hydrochloric acid
3. 3
   건조dried over anhydrous sodium sulfate
4. 4
   workup.DISTILLATIONthe solvent was distilled off
5. 5
   세척residue was washed with n-hexane
6. 6
   기타dried
7. 7
   기타to give a crude end product

실험 절차

10 Grams of p-hydroxybenzoic acid and 15 g of decanoic acid chloride were stirred at room temperature, and 7.2 g of pyridine was dropwise added. After the mixture was stirred for 1 day, a reaction product was poured into water, and an organic layer was extracted with dichloromethane. The organic layer was washed with 1N hydrochloric acid and dried over anhydrous sodium sulfate, the solvent was distilled off, and then residue was washed with n-hexane and then dried to give a crude end product.

출처