반응 #847

반응 방정식

thionyl chloride

p-octyloxybenzoic acid

( 1 )

p-n-octyloxybenzoic acid

→

4-octyloxybenzoic acid chloride

반응 조건

후처리

1. 1
   온도the mixture was refluxed for 5 hours
2. 2
   workup.DISTILLATIONExcessive thionyl chloride was distilled off
3. 3
   기타to give a crude end compound

실험 절차

A large excess of thionyl chloride was added to 10 g of the p-octyloxybenzoic acid prepared in (1), and the mixture was refluxed for 5 hours. Excessive thionyl chloride was distilled off to give a crude end compound.

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