반응 #8428

ord-1709dad3b5804316bd81b6fe75a13e7a

반응 방정식

Cc1ccccc1S(=O)(=O)n1ccc2c(Br)cccc21
4-bromo-1-(2-methyl-benzenesulfonyl)-1H-indole
C1CNCCN1
piperazine
Cc1ccccc1S(=O)(=O)n1ccc2c(N3CCNCC3)cccc21
title compound
Cc1ccccc1S(=O)(=O)n1ccc2c(N3CCNCC3)cccc21
4-(1-Piperazinyl)-1-(2-methylbenzenesulfonyl)-1H-indole

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

The title compound was prepared from 4-bromo-1-(2-methyl-benzenesulfonyl)-1H-indole and piperazine according to Method 1 to give 25 mg (12%) of a white solid: 1HNMR (CD3OD) δ 7.91–6.79 (m, 9H), 3.49–3.30 (m, 8H), 2.48 (s, 3H); MS (ESI) 356.1 (M+H)+; Purity (HPLC) >95%.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07087750B2uspto-grants-2006_08