반응 #84231

ord-b3bcd0e62c59493796e86dfc933a3281

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타This compound was prepared

실험 절차

This compound was prepared using the standard Sonagashira procedure as described in General Procedures Example C, reacting from N-(4-chloro-2-iodo-5-trifluoromethyl-phenyl)-methanesulfonamide (0.60 g, 1.5 mmol) and 3-(2,2,2-Trifluoro-ethylsulfanylmethyl)-pent-1yn-3-ol (0.32 g, 1.5 mmol) to yield the title compound as a yellow sticky oil.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US09434688B2uspto-grants-2016_09