반응 #84228

ord-d9c0f36b6a864549b8405a1fb429a6f4

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타This compound was prepared

실험 절차

This compound was prepared using the standard de-protection procedure, as described in General Procedure Example B, starting from 2-(1-methanesulfonyl-5-nitro-6-trifluoromethyl-1H-indol-2-yl)-1-(2,2,2-trifluoro-ethylsulfanyl)-butan-2-ol (0.65 g, 1.31 mmol) and using 4N sodium hydroxide as base (1 mL, 4.0 mmol) to yield the title compound as a solid.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US09434688B2uspto-grants-2016_09