반응 #84219

ord-963e13d4739c4aaeb3f0eeb94d3d99d9

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타This compound was prepared

실험 절차

This compound was prepared using the general Sonagashira conditions as described in general Example C, starting from N-(2-iodo-4-nitro-5-trifluoromethyl-phenyl)-methanesulfonamide (9.0 g, 21.9 mmol) and 2-methyl-1-buten-3-yne (6.25 mL, 65.7 mmol) to yield the title compound as a reddish-brown solid.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US09434688B2uspto-grants-2016_09