반응 #8416
ord-cf519e59ac3e498dbf8b96e2bf5828fe
반응 방정식
4-(4-boc-piperazinyl)-indole
4-methoxyphenylsulfonyl chloride
→
title compound
1-[(4-Methoxyphenyl)sulfonyl]-4-(1-piperazinyl)-1H-indole Hydrochoride
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
The title compound was prepared from 4-(4-boc-piperazinyl)-indole and 4-methoxyphenylsulfonyl chloride according to Method 3: 1H NMR (270 MHz, DMSO-d6) δ 9.07 (br, 1 H), 7.90 (d, J=8 Hz, 2 H), 7.78 (d, J=5 Hz, 1 H), 7.61 (d, J=8 Hz, 1 H), 7.25 (t, J=8 Hz, 1 H), 7.09 (d, J=8 Hz, 2 H), 6.92 (d, J=5 Hz, 1 H), 6.68 (d, J=8 Hz, 1 H), 3.79 (s, 3 H), 3.24 (m, 8 H); MS (ESI+) for m/z 371 (M+H)+.