반응 #84025

ord-d872591027264a99a4c357f08f23f73a

반응 방정식

O=C(Cl)C(=O)Cl
Oxalyl chloride
CC(C)(C)O
t-butyl alcohol
CC(C)(C)OC(=O)C(=O)Cl
Compound 34
CC(C)(C)OC(=O)C(=O)Cl
Chloro-Oxo-Acetic Acid t-Butyl Ester

시약

없음

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The solvent was evaporated under vacuum

실험 절차

Oxalyl chloride (232 μL, 2.8 mmol) and t-butyl alcohol (228 μL) were combined in ether (6.7 mL) under nitrogen at 0° C. The resulting mixture was stirred for 30 minutes at room temperature. The solvent was evaporated under vacuum to form Compound 34.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US09433598B2uspto-grants-2016_09