반응 #83410

반응 방정식

meta-trifluoromethylphenol

sodium hydride

2-chloro-6-(3-thienylmethyloxy)-4-trifluoromethylpyridine

→

2-(3-thienylmethyloxy)-4-trifluoromethyl-6-(meta-trifluoromethylphenoxy)pyridine

용매

dimethylformamide

반응 조건

후처리

1. 1
   기타To a mixture prepared
2. 2
   workup.ADDITIONwas added

실험 절차

To a mixture prepared by adding to meta-trifluoromethylphenol (1.1 g, 0.0034×2.0 mol) successively dimethylformamide and sodium hydride (0.20 g, (ca.60% in mineral oil), 0.0034×1.5 mol), 2-chloro-6-(3-thienylmethyloxy)-4-trifluoromethylpyridine (1.0 g, 0.0034 mol) was added, and the resultant solution was refluxed for about 2 hours.

출처