반응 #83405

반응 방정식

3-thiophenemethanol

sodium hydride

2,6- dichloro-4-methoxypyridine

→

2-chloro-4-methoxy-6-(3-thienylmethyloxy)pyridine

용매

tetrahydrofuran

반응 조건

후처리

1. 1
   workup.ADDITIONwas added

실험 절차

To a solution containing 3-thiophenemethanol (0.45 g, 0.0033×1.2 mol) and sodium hydride (0.14 g, (ca.60% in mineral oil), 0.033×1.05 mol) in tetrahydrofuran, 2,6- dichloro-4-methoxypyridine (0.59 g, 0.0033 mol) was added and the resultant solution was refluxed for about 2 hours.

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