반응 #833563

반응 방정식

tert-butyl hydrazinecarboxylate

phenylvinylsulphone

→

Tert-butyl N′-(2-phenylsulphonyl-ethyl)-hydrazinecarboxylate

용매

ethanol

반응 조건

후처리

1. 1
   기타Then the solvent is removed completely
2. 2
   기타the residue is chromatographed over silica gel (cyclohexane/ethyl acetate)

실험 절차

A solution of 0.79 g tert-butyl hydrazinecarboxylate and 1.00 g phenylvinylsulphone in 8 ml of ethanol is refluxed for 5 h with stirring. Then the solvent is removed completely and the residue is chromatographed over silica gel (cyclohexane/ethyl acetate).

출처