반응 #833561

반응 방정식

2-quinolinecarboxaldehyde

tert-butyl hydrazinecarboxylate

→

Tert-butyl N′-(quinolin-2-yl)methylene-hydrazine carboxylate

용매

ethanol

반응 조건

후처리

1. 1
   기타Then the solution is evaporated to dryness
2. 2
   기타the residue is triturated with diisopropylether
3. 3
   기타separated off
4. 4
   기타dried at 50° C.

실험 절차

A solution of 10.70 g 2-quinolinecarboxaldehyde and 9.00 g tert-butyl hydrazinecarboxylate in 200 ml of ethanol is refluxed for 2 h with stirring. Then the solution is evaporated to dryness and the residue is triturated with diisopropylether, separated off and dried at 50° C.

출처