반응 #833510

반응 방정식

Vanillin

allyl bromide

potassium carbonate

→

3-methoxy-4-(2-propenyloxy)benzaldehyde

용매

acetone

반응 조건

후처리

1. 1
   온도After cooling
2. 2
   여과the solid was filtered off
3. 3
   세척washed with acetone
4. 4
   기타A yellow oil was obtained
5. 5
   농축after a thorough concentration of the organic phases

실험 절차

Vanillin (20.0 g, 0.130 mol) and allyl bromide (19.9 g, 0.160 mol) were heated under reflux together with potassium carbonate (27.3 g, 0.200 mol) in 150 ml acetone (abs.) for 8 hours. After cooling, the solid was filtered off and washed with acetone. A yellow oil was obtained after a thorough concentration of the organic phases.

출처