반응 #8315

반응 방정식

3-benzyl-4-bromo-butyric acid

thionyl chloride

→

3-benzyl-4-bromo-butyryl chloride

수율 127.0%

반응 조건

후처리

1. 1
   기타The thionyl chloride is evaporated

실험 절차

A mixture of 3-benzyl-4-bromo-butyric acid (2.0 g, 7.78 mmol) and thionyl chloride (6.0 mmol) is heated to 80° C. for 2 h. The thionyl chloride is evaporated to yield 3-benzyl-4-bromo-butyryl chloride 2.1 g (99%), as a colorless liquid.

출처