반응 #831123

ord-167f2ffa4b864eb78eb65bbfce170eed

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타the polymerization
  2. 2
    기타as described in Synthesis Example 1, (1),

실험 절차

Using p-tert-butoxystyrene (83.7 g, 0.475 mole) and p-chlorostyrene (3.5 g, 0.025 mole), the polymerization and the treatment were carried out in the same manner as described in Synthesis Example 1, (1), to give 75.9 g of poly(p-tert-butoxystyrene/p-chlorostyrene) as white powder having Mw 22000 (GPC with polystyrene calibration). The polymer was found to have p-tert-butoxystyrene unit and p-chlorostyrene unit in a molar ratio of ca. 95:5 based on 1HNMR.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05558976uspto-grants-1996_09