반응 #831123
ord-167f2ffa4b864eb78eb65bbfce170eed
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타the polymerization
- 2기타as described in Synthesis Example 1, (1),
실험 절차
Using p-tert-butoxystyrene (83.7 g, 0.475 mole) and p-chlorostyrene (3.5 g, 0.025 mole), the polymerization and the treatment were carried out in the same manner as described in Synthesis Example 1, (1), to give 75.9 g of poly(p-tert-butoxystyrene/p-chlorostyrene) as white powder having Mw 22000 (GPC with polystyrene calibration). The polymer was found to have p-tert-butoxystyrene unit and p-chlorostyrene unit in a molar ratio of ca. 95:5 based on 1HNMR.