반응 #831122

ord-29f23abe28db4c17809077837d1478fa

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타the polymerization and treatment
  2. 2
    기타as described in Synthesis Example 1, (1),

실험 절차

Using p-tert-butoxystyrene (77.6 g, 0.44 mole) and p-methoxystyrene (8.1 g, 0.06 mole), the polymerization and treatment were carried out in the same manner as described in Synthesis Example 1, (1), to give 77.1 g poly(p-tert-butoxystyrene/p-methoxystyrene) as white powder having Mw 20000 (GPC with polystyrene calibration). The polymer was found to have p-tert-butoxystyrene unit and p-methoxystyrene unit in a molar ratio of ca. 88:12 based on 1HNMR.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05558976uspto-grants-1996_09