반응 #831120

ord-d335ec40c69c4205bb30040a5d145a33

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타the polymerization
  2. 2
    기타as described in Synthesis Example 1, (1),

실험 절차

Using p-tert-butoxystyrene (81.1 g, 0.46 mole) and styrene (4.6 g, 0.04 mole), the polymerization and the treatment were carried out in the same manner as described in Synthesis Example 1, (1), to give 77.1 g of poly(p-tert-butoxystyrene/styrene) as white powders having Mw 20000 (GPC with polystyrene calibration). The polymer was found to have p-tert-butoxystyrene unit and styrene unit in a molar ratio of ca. 92:8 based on 1HNMR.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05558976uspto-grants-1996_09