반응 #830422
ord-f5a6f365467b4f26a2b48a2a3246e0b3
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1농축The reaction mixture was then concentrated by evaporation under reduced pressure
- 2기타dried in vacuo
실험 절차
Following a procedure similar to that described in Example 1(c), 450 mg of 1-methyl-2-{2-[2-(4-phenylbutyl)phenoxy]ethyl}piperidine [prepared as described in step (a) above] dissolved in 5 ml of ethyl acetate were converted to the hydrdochloride by treating it with 0.4 ml of a 4N solution of hydrogen chloride in dioxane. The reaction mixture was then concentrated by evaporation under reduced pressure and dried in vacuo, to give 496 mg of the title compound as a colorless oil.