반응 #830420
ord-895a9fea50b34cfea0b7205a25fe6ae1
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1workup.DISTILLATIONAt the end of this time, the reaction mixture was freed from the solvent by distillation under reduced pressure
- 2세척The resulting residue was washed with hexane
- 3기타dried in vacuo
실험 절차
10 ml of a 4N solution of hydrogen chloride in dioxane were added to a solution of 1.13 g of 1-t-butoxycarbonyl-2-{2-[2-(4-phenylbutyl)phenoxy]ethyl}piperidine [prepared as described in step (b) above] in 10 ml of dioxane, and the resulting mixture was stirred at room temperature for 30 minutes. At the end of this time, the reaction mixture was freed from the solvent by distillation under reduced pressure. The resulting residue was washed with hexane and dried in vacuo, to give 0.94 g (yield 97%) of the title compound as a colorless oil.