반응 #828717

ord-124348c9e3c74a01bcdfa140f15247e0

반응 방정식

CCOC(C)=O
ethyl acetate
N[C@@H](CCc1ccccc1)C(=O)O
L-HPA
N[C@H](CCc1ccccc1)C(=O)O
D-homophenylalanine

시약

없음

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타After the completion of the reaction
  2. 2
    기타After separating the lower layer from the upper layer
  3. 3
    기타to obtain D-HPAE, which

실험 절차

After the completion of the reaction, an extractant such as ethyl acetate is added to the reaction mixture which separates the reaction mixture into an upper layer and a lower layer. The upper layer contains D-HPAE in the organic solvent and the lower layer contains L-HPA in water. After separating the lower layer from the upper layer, the extractant, i.e., ethyl acetate, can be vaporized to obtain D-HPAE, which can be chemically hydrolyzed to obtain D-homophenylalanine.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05552317uspto-grants-1996_09