반응 #828712
ord-9595334a782f420e929bf7c210e29da7
반응 방정식
9-borabicyclo[3.3.1]nonane
HCl
→
title compound
수율 75.0%
B-chloro-9-borabicyclo[3.3.1]nonane
수율 75.0%
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
The title compound was prepared in 75% yield following the method of Example 1 by treating 9-borabicyclo[3.3.1]nonane (9-BBN, Aldrich Chemical Company, Inc., Milwaukee, Wis.) with anhydrous HCl in ether. 11B NMR δ 79 ppm in hexane, bp 65° C. (0.3 mm).