반응 #82417

반응 방정식

2-(2',3'-dimethoxyphenyl)-1-furanylethanone

hydrogen

hydrogen

→

title compound

수율 70.5%

2-(2',3'-Dimethoxyphenyl)-1-tetrahydrofuranyl Ethanol

수율 70.5%

용매

methanol

반응 조건

후처리

1. 1
   여과The solution was filtered
2. 2
   농축concentrated in vacuo

실험 절차

A solution of 450 mg(1.8 mmol) of 2-(2',3'-dimethoxyphenyl)-1-furanylethanone, from Step 2, and 20% palladium on carbon (225 mg) in 75 mL of methanol was shaken under 4 atmospheres of hydrogen until hydrogen uptake ceased. The solution was filtered and concentrated in vacuo to give 320 mg (69% yield) of the title compound as an oily solid. This product was carried on without purification to the next step.

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