반응 #82335

반응 방정식

N2 (benzyloxycarbonyl)-N1 -isopentyl-L-prolinamide

→

N1 -isopentyl-L-prolinamide

수율 111.5%

용매

ethanol

반응 조건

후처리

1. 1
   기타The catalyst was removed by filtration
2. 2
   기타the filtrate was evaporated

실험 절차

A solution of 5.73 g of N2 -(benzyloxycarbonyl)-N1 -isopentyl-L-prolinamide in 600 ml of ethanol was hydrogenated over 0.8 g of 10% palladium-on-carbon catalyst for 3.75 hours. The catalyst was removed by filtration and the filtrate was evaporated to give 3.4 g of N1 -isopentyl-L-prolinamide as an oil which was used without further purification.

출처