반응 #82144
ord-165c21acb8a34d9c9681683a969f54e5
시약
없음
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1여과The polymer was filtered
- 2추출The ground material was extracted with 2-propanol for 24 hrs in a Soxhlet extractor
- 3기타dried
- 4기타to afford a pale brown solid which
실험 절차
The resulting heterogeneous reaction mixture, which was lumpy and hardened, was neutralized by addition of 15% aqueous tartaric acid solution. The polymer was filtered and a small portion was ground thoroughly. The ground material was extracted with 2-propanol for 24 hrs in a Soxhlet extractor and dried to afford a pale brown solid which was not soluble to any extent in distilled water.