반응 #81965

반응 방정식

4-mercapto-2-phenyl-pyrimidine-5-carboxylic acid phenethyl-amide

iodine

→

title compound

수율 71.5%

2-Phenethyl-6-phenyl-isothiazolo[5,4-d]pyrimidin-3-one

수율 71.5%

반응 조건

실험 절차

Using the procedure of Example 20, 2.0 g (5.96 mmol) of 4-mercapto-2-phenyl-pyrimidine-5-carboxylic acid phenethyl-amide were treated with 1.66 g (6.56 mmol) of iodine to give 1.42 g of the title compound after recrystallization from isopropanol, mp 144°-147° C.

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