반응 #816374
ord-91979d10fc6f470b8efe5d56b30768d7
반응 방정식
4-amino-1,5-dimethyl-2-phenyl-1,2-dihydro-3H-pyrazol-3-one
o-cresol
ammonia
→
1,5-dimethyl-4-{[(1Z)-3-methyl-4-oxocyclohexa-2,5-dien-1-ylidene]amino}-2-phenyl-1,2-dihydro-3H-pyrazol-3-one
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타ranging from 5 to 10° C.
실험 절차
10 mmol of 4-amino-1,5-dimethyl-2-phenyl-1,2-dihydro-3H-pyrazol-3-one was dissolved in 30 ml of water. This solution was admixed with 10 mmol of o-cresol in solution in 30 ml of 2-propanol, 3 ml of 20% aqueous ammonia and 22 mmol of potassium ferricyanide at a temperature ranging from 5 to 10° C.