반응 #81073

반응 방정식

3,5-di-t-butylbenzoic acid

nitric acid

thionyl chloride

→

3,5-Di-t-butyl-2-nitrobenzoyl chloride

3,5-di-t-butyl-2-nitrobenzoic acid

용매

dimethylformamide

반응 조건

실험 절차

3,5-Di-t-butyl-2-nitrobenzoyl chloride was prepared by nitration of 3,5-di-t-butylbenzoic acid 46.86 grams (0.20 mol) with 90% nitric acid (150 ml, d=1.5) to give 3,5-di-t-butyl-2-nitrobenzoic acid (54.6 grams) followedby treatment with thionyl chloride (250 ml) with dimethylformamide (1 ml).

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