반응 #806960

ord-de08b7d99de849f58abb883cc1e58255

반응 방정식

COc1ccccc1NS(C)(=O)=O
N-(2-methoxyphenyl)methanesulfonamide
O=C(Cl)CCCCCBr
6-bromohexanoyl chloride
→
COc1ccc(C(=O)CCCCCBr)cc1NS(C)(=O)=O
title compound
COc1ccc(C(=O)CCCCCBr)cc1NS(C)(=O)=O
N-[5-(6-Bromohexanoyl)-2-methoxyphenyl]methanesulfonamide

반응물

COc1ccccc1NS(C)(=O)=O
N-(2-methoxyphenyl)methanesulfonamide
O=C(Cl)CCCCCBr
6-bromohexanoyl chloride

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Using N-(2-methoxyphenyl)methanesulfonamide (10.0 g) and 6-bromohexanoyl chloride (8.37 ml) according to the same method as that of Reference Example 1, the title compound (9.80 g) was obtained as colorless crystals.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07132547B2uspto-grants-2006_11