반응 #806269

반응 방정식

triethylammonium 2-(6-cyano-1-hexyn-1-yl)adenosine 5′-monophosphate

HCl

→

2-(6-cyano-1-hexyn-1-yl)adenosine 5′-monophosphate

용매

water

water

반응 조건

후처리

1. 1
   workup.ADDITIONwas added
2. 2
   여과the resultant mixture was filtered
3. 3
   세척The residue was washed with water (20 mL)

실험 절차

A triethylammonium 2-(6-cyano-1-hexyn-1-yl)adenosine 5′-monophosphate (1.1 g) was dissolved in water (20 mL), and, under ice-cooling conditions, 1N HCl solution (2 mL) was added thereto, followed by standing for 10 minutes. After having been diluted with water (20 mL), the resultant mixture was filtered. The residue was washed with water (20 mL) and then with ethanol (20 mL×2), to thereby yield 617 mg of the above-titled compound as a colorless amorphous substance.

출처