반응 #806243

ord-1692dc1ed806452ca7382107d965b1e2

반응 방정식

Oc1ccccc1
phenol
O=S(=O)(O)O
sulfuric acid
O=S(=O)(O)O
sulfuric acid
O=S(=O)(O)O
sulfuric acid
Oc1ccccc1
Phenol
Oc1ccccc1
phenol
Oc1ccccc1
phenol
Oc1ccccc1
Phenol
O=S(=O)(O)c1ccc(O)cc1
phenolsulfonic acid

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타A facial exfoliant was prepared

실험 절차

A facial exfoliant was prepared. A solution of phenolsulfonic acid was prepared as described in Example 1, except that the weight of available stock liquefied phenol USP was calculated and prepared for 4.0 moles of phenol. The amount of available stock sulfuric acid NF that contained 4.0 moles was calculated. The weight of sulfuric acid NF was 392.32 grams. The 4.0 moles of sulfuric acid NF was treated as described in Example 1. A quantity of 400 mL of Liquified Phenol USP was added to a 600 mL beaker. A quantity of 4.0 moles of phenol as Liquefied Phenol USP was added to a 1 L Corning Pyrex No. 1395 bottle using the Mettler PS-5002-S balance.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07132111B2uspto-grants-2006_11