반응 #80342

ord-94d57286b70b47c4a745d79789fc8988

반응 방정식

NC/C=C\COc1cc(CN2CCCCC2)ccn1
4-(4-piperidinomethyl-2-pyridyloxy) -cis-2-butenylamine
O=C(O)c1ccco1
2-furancarboxylic acid
O=C(NC/C=C\COc1cc(CN2CCCCC2)ccn1)c1ccco1
title compound
수율 82.0%
O=C(NC/C=C\COc1cc(CN2CCCCC2)ccn1)c1ccco1
N-[4-(4-Piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]furan-2-carboxamide
수율 82.0%

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Following a procedure similar to that described in Example 13, but using 4-(4-piperidinomethyl-2-pyridyloxy) -cis-2-butenylamine and 2-furancarboxylic acid as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained as an oil in an 82% yield.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05616579uspto-grants-1997_04