반응 #78410
ord-ed221a40b0554bbd900e864b34ebf7eb
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타The derivative was synthesized
- 2온도cooled with ice
실험 절차
The derivative was synthesized as follows. 20 grams of the derivative of acrylate obtained as the third example was dissolved in 20 milliliters of toluene. 7 grams of cyclopentadiene was dropped into the solution cooled with ice, and was agitated through all night. Dicyclopentadiene was produced as by-product, and was eliminated in vacuum. Then, 24.9 grams of the derivative of norbornene was obtained. The derivative of norbornene was viscous liquid, and the yield was 95%.