반응 #78034

ord-8b36773a880f40459c48d159426a9457

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Starting from 7-chloro-9,10-dihydropyrrolo[2,1-b][1,3]benzothiazepin-9-one (0.19 g, 0.76 mmol) and N-ethylpiperazine (0.70 mL, 6.13 mmol), the title compound was obtained following the above described procedure for (1). After purification, 0.19 g of the desired product were obtained as a white solid (yield 74%).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06710041B2uspto-grants-2004_03