반응 #77854

반응 방정식

N-(3-{5-[3-(formamido)prop-1-ynyl]pyridin-2-yl}prop-2-ynyl)formamide

N-(3-{5-[3-(Formamido)prop-1-ynyl]pyridin-2-yl}prop-2-ynyl)formamide

→

13-1

N-(3-{5-[3-(Formylamino)propyl]pyridin-2-yl}propyl)formamide

용매

methanol

반응 조건

후처리

1. 1
   여과The mixture was filtered through Solka Floc
2. 2
   농축The filtrate was concentrated

실험 절차

A mixture of N-(3-{5-[3-(formamido)prop-1-ynyl]pyridin-2-yl}prop-2-ynyl)formamide (9-1) (28 g) and 5% Pd/Al2O3 (2.8 g) in methanol (350 mL) was hydrogenated at 40 psi at ambient temperature for 5 h. The mixture was filtered through Solka Floc. The filtrate was concentrated to afford 13-1 as an oil.

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