반응 #76691

ord-af508c38ec2e46b0b21b9ae390a29200

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The product obtained
  2. 2
    기타was purified by silica gel chromatography (hexane:ethyl acetate=1:1)

실험 절차

Using 4-chloro-5-(2-thienyl)thieno[2,3-d]pyrimidine (50 mg, 0.20 mmol) and 2-aminoindan (110 mg, 0.80 mmol), a similar procedure to Production Example 190 was carried out. The product obtained was purified by silica gel chromatography (hexane:ethyl acetate=1:1) to obtain the title compound (70 mg, 0.20 mmol) having the following physical properties:

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06703421B1uspto-grants-2004_03