반응 #76686

반응 방정식

2-chloro-1-thia-2,3,5,7-tetraazaindene

2-aminoindan

→

title compound

수율 51.7%

2-(2-Indanylamino)-1-thia-2,3,5,7-tetraazaindene

수율 51.7%

반응 조건

후처리

1. 1
   기타The product obtained
2. 2
   기타was purified by silica gel chromatography (hexane:ethyl acetate=3:1)

실험 절차

Using 2-chloro-1-thia-2,3,5,7-tetraazaindene (50 mg, 0.29 mmol) (see J. Org. Chem. 26, 4961 (1961), J. Chem. Soc. (C) 1856 (1967)) and 2-aminoindan (120 mg, 0.90 mmol), a similar procedure to Production Example 190 was carried out. The product obtained was purified by silica gel chromatography (hexane:ethyl acetate=3:1) to obtain the title compound (41 mg, 0.15 mmol) having the following physical properties:

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