반응 #7650

ord-f76a8a8b48e24cfcac66d166cb5a1dec

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The crude product is used in the next step without further purification

실험 절차

In analogy to the procedure for Example 36A, 150 mg (0.67 mmol) 6-(1-aminopropyl)-3-cyclopentyl-1,2,4-triazin-5(4H)-one, 120 mg (0.74 mmol) bicyclo[2.2.1]hept-5-ene-2-carbonyl chloride and proportionate amounts of the other reagents are used. The crude product is used in the next step without further purification.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07087605B2uspto-grants-2006_08