반응 #76376
ord-2d89c4a6c19742cea11d66a9ead29487
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타quenched with water
- 2추출extracted with ethyl acetate:hexane (1:1)
- 3세척washed with brine, over MgSO4
- 4농축concentrated in vacuo
실험 절차
To the commercially available 6-bromo-naphthalene-2-ol (1) (1 equi.) and benzyl bromide (2) (1 equi.) in DMF (3mL/mmole), cesium carbonate (1.25 equi.) was added at room temperature. The reaction mixture was stirred at that temperature for 24 h, quenched with water, extracted with ethyl acetate:hexane (1:1), washed with brine, over MgSO4, and concentrated in vacuo.