반응 #7637

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6-(1-aminopropyl)-3-cyclopropyl-1,2,4-triazin-5(4H)-one

cyclobutanecarbonyl chloride

→

N-[1-(3-Cyclopropyl-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl)propyl]cyclobutanecarboxamide

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후처리

1. 1
   기타The crude product is used in the next step without further purification

실험 절차

In analogy to the procedure for Example 36A, 250 mg (1.29 mmol) 6-(1-aminopropyl)-3-cyclopropyl-1,2,4-triazin-5(4H)-one, 150 mg (1.29 mmol) cyclobutanecarbonyl chloride and proportionate amounts of the other reagents are used. The crude product is used in the next step without further purification.

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