반응 #7606
ord-3530e699346948b5a62efd1270abe4aa
반응 방정식
acetylchloride
2-amino-thiazole
tert.-butylisonitrile
benzaldehyde
→
7-acetyl-5-tert-butylamino-6-phenyl-imidazo[2,1-b]-thiazol-7-ium chloride
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
Example 4 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-thiazole (0.1 M, DCM), 0.575 ml (0.115 mmol) tert.-butylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) benzaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.