반응 #75652
ord-a143d2b5e5ac4c2996929dc839306c84
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
Compound 20 was prepared by the basic process from 5.0 mmol 3,5-dichloroaniline, 5.5 mmol ethylglyoxalate solution (50% toluene), 15.0 mmol 4-methylstyrene and 5.0 mmol trifluoroacetic acid in 30.0 ml acetonitrile. Subsequent saponification was carried out using 1.0 ml of sodium hydroxide solution (6N water) in 20.0 ml of ethanol.