반응 #75460
ord-4b15037d83db4e43bf5c3e0a1adac34f
반응 방정식
nitric acid
arachidic acid
stearic acid
sodium hydroxide
→
sodium behenate
반응 조건
온도
55°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1workup.STIRRINGstirred for 30 minutes
실험 절차
In an amount of 32.4 g of behenic acid, 9.9 g of arachidic acid and 5.6 g of stearic acid were dissolved in 945 mL of pure water at 90° C. Then, the solution was added with 98 mL of 1.5 mol/L sodium hydroxide aqueous solution with stirring at high speed. Subsequently, the solution was added with 0.93 mL of concentrated nitric acid, cooled to 55° C. and stirred for 30 minutes to obtain a sodium behenate solution.